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Fixed-point calibration

Instruments calibrated

Standard Platinum Resistance Thermometers (SPRT) and thermocouples, types S and R.

Temperature range for SPRT

–189.3442 °C to 660.323 °C

–190 °C to 0 °C: triple points of argon, mercury and water
–190 °C to 420 °C: triple points of argon, mercury, water; freezing points of tin and zinc
–190 °C to 660 °C: triple points of argon, mercury, water; freezing points of tin, zinc and aluminium
–39 °C to 30 °C: triple points of mercury and water; melting point of gallium
0 °C to 30 °C: triple point of water and melting point of gallium
0 °C to 157 °C: triple point of water and freezing point of indium
0 °C to 232 °C: triple point of water; freezing points of indium and tin
0 °C to 420 °C: triple point of water; freezing points of tin and zinc
0 °C to 660 °C: triple point of water; freezing points of tin, zinc and aluminium

Measurement uncertainty for SPRT

The measurement uncertainty depends on the thermometer being calibrated. Uncertainty is expressed as an interval which, assuming a normal distribution, corresponds to a confidence level of approximately 95% (k = 2).

Method

Calibration is performed by determining the thermometer resistance R(t) at the respective fixed points by comparison with the laboratory’s reference resistors. The thermometer’s W-values at the fixed points are stated in the calibration certificate and are used to calculate the constants of the interpolation formula.
W is defined as:

W = R(t) / R(0.01 °C)

Our best measurement capability

Temperature range for thermocouples: 0 °C to 1100 °C

230 °C to 1100 °C: freezing points of tin, zinc, aluminium, silver and copper
230 °C to 962 °C: freezing points of tin, zinc, aluminium and silver
230 °C to 660 °C: freezing points of tin, zinc and aluminium
230 °C to 420 °C: freezing points of tin and zinc

Measurement uncertainty for thermocouples

Typical measurement uncertainty for a Type S thermocouple (Pt–Pt/10%Rh) is 0.2 °C to 0.3 °C (2 standard deviations).

Method

Calibration is performed by measuring the thermoelectric voltage generated when one junction of the thermocouple is placed at the metal’s freezing plateau temperature, while the other is maintained at 0.00 °C.

Traceability diagram

 

Contact information

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